Microwave extraction is an innovative technique used in sample preparation. It represents a significant advancement over conventional extraction methods and is considered a green, eco-friendly technology that supports sustainable practices. This paper provides an overview of the underlying principles, key features, equipment, and operational parameters of microwave extraction. In particular, it highlights its growing application and recent developments in the pretreatment of soil and sediment samples over the past ten years. The technology has gained increasing attention due to its efficiency, reduced solvent use, and shorter processing times. As environmental concerns continue to rise, microwave extraction offers a promising alternative that aligns with modern analytical requirements while minimizing ecological impact. This review aims to serve as a valuable reference for researchers and practitioners working in environmental analysis and sample preparation.
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